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AUTONOMOUS  UNIVERSITY  OF  MADRID   DEPARTMENT  OF  MOLECULAR  BIOLOGY    

   

Inflammation  and  Skin  Cancer  Mediated     Through  c-­Fos/AP-­1  

   

EVA  MARÍA  BRISO  DE  MONTIANO  

               

MADRID,  2013  

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 AUTONOMOUS  UNIVERSITY  OF  MADRID   FACULTY  OF  SCIENCES  

DEPARTMENT  OF  MOLECULAR  BIOLOGY    

Inflammation  and  Skin  Cancer  Mediated     Through  c-­Fos/AP-­1  

 

Doctoral  thesis  submitted  to  the  Autonomous  University  of  Madrid       for  the  degree  of  Doctor  of  Philosophy  by  

M.Sci.  in  Molecular  Biomedicine,   Eva  María  Briso  de  Montiano  

 

Thesis  Director  

Prof.  Dr.  Erwin  F.  Wagner    

   

GENES,  DEVELOPMENT  AND  DISEASE  GROUP   F-­BBVA-­CANCER  CELL  BIOLOGY  PROGRAMME   SPANISH  NATIONAL  CANCER  RESEARCH  CENTRE  

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This  thesis,  submitted  for  the  degree  of  Doctor  of  Philosophy  at  the  Autonomous   University  of  Madrid,  has  been  completed  in  the  Genes,  Development  and  Disease  

Laboratory  a  the  Spanish  National  Cancer  Research  Centre  (CNIO),  under  the   supervision  of  Prof.  Dr.  Erwin  F.  Wagner  

   

           

This  work  was  supported  by  the  following  grants  and  fellowships:  

 La  Caixa/CNIO  International  PhD  Fellowship.  2008  Call.  Eva  Briso  de  Montiano  

 ERC  Advanced  Grant:  Erwin  F.  Wagner  

 Fundación  Banco  Bilbao  Vizcaya  (F-­‐BBVA)  -­‐  CNIO  Cancer  Cell  Biology  Program    

       

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As  you  set  out  for  Ithaka   hope  your  road  is  a  long  one,   full  of  adventure,  full  of  discovery.  

Laistrygonians,  Cyclops,  

angry  Poseidon—don’t  be  afraid  of  them:  

you’ll  never  find  things  like  that  on  your  way   as  long  as  you  keep  your  thoughts  raised  high,   as  long  as  a  rare  excitement  

stirs  your  spirit  and  your  body.  

Laistrygonians,  Cyclops,  

wild  Poseidon—you  won’t  encounter  them   unless  you  bring  them  along  inside  your  soul,   unless  your  soul  sets  them  up  in  front  of  you.  

 

Hope  your  road  is  a  long  one.  

May  there  be  many  summer  mornings  when,   with  what  pleasure,  what  joy,  

you  enter  harbors  you’re  seeing  for  the  first  time;  

may  you  stop  at  Phoenician  trading  stations   to  buy  fine  things,  

mother  of  pearl  and  coral,  amber  and  ebony,   sensual  perfume  of  every  kind—  

as  many  sensual  perfumes  as  you  can;  

and  may  you  visit  many  Egyptian  cities  

to  learn  and  go  on  learning  from  their  scholars.  

 

Keep  Ithaka  always  in  your  mind.  

Arriving  there  is  what  you’re  destined  for.  

But  don’t  hurry  the  journey  at  all.  

Better  if  it  lasts  for  years,  

so  you’re  old  by  the  time  you  reach  the  island,   wealthy  with  all  you’ve  gained  on  the  way,   not  expecting  Ithaka  to  make  you  rich.  

 

Ithaka  gave  you  the  marvelous  journey.  

Without  her  you  wouldn't  have  set  out.  

She  has  nothing  left  to  give  you  now.  

And  if  you  find  her  poor,  Ithaka  won’t  have  fooled  you.    

Wise  as  you  will  have  become,  so  full  of  experience,   you’ll  have  understood  by  then  what  these  Ithakas  mean.  

 

Ithaka.  KP  Kavafis  

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Dedicated  to  my  family   In  memory  of  my  grandmother    

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  A cknowledgements  

     

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  This  doctoral  thesis  is  the  result  of  my  research  spanning  the  past  four  years  of   my  life  and  would  not  have  been  possible  without  the  aid,  support  and  contribution  of   many  people  to  whom  I  wish  to  express  my  gratitude  here.  

    I  want  to  thank  Dr.  Erwin  Wagner  for  giving  me  the  great  opportunity  to  carry   out  my  PhD  in  his  group,  as  well  for  scientific  guidance,  discussion  of  my  project  and  for   allowing  me  to  meet  internationally  recognized  scientists  and  discuss  my  project  with   them.  

  Very  special  thanks  to  Dr.  Juan  Guinea-­‐Viniegra,  not  only  for  beeing  a  very  good   friend  of  mine  but  also  for  his  unconditional  support,  scientific  guidance,  his  patience,   for  reviewing  this  thesis  and  for  everything  you  have  taught  me    during  my  PhD.        

  I   am   very   grateful   to   all   the   members   of   the   Genes,   Development   and   Disease   group  and  the  CCB  Program,  for  creating  an  inspiring  atmosphere  in  the  lab.  Especially,  I   want  to  thank  my  neighbors,  Francy  and  Jochen,  for  those  fun  moments  we  spent  while   pipetting,  Marta  and  María  Martín  for  your  help  prepping  the  tails.  I  want  to  thank  María   Jiménez  and  Ana  Guio  for  organizing  the  lab.    

  I  want  to  thank  Dr.  Mercedes  Rincón  because  of  the  big  support  and  motivation   you  have  given  me.  I  admire  your  passion  and  dedication  to  science.  Above  all,  because   my  interest  for  science  started  in  your  lab  when  I  was  still  an  undergraduate  student  at   the  University  of  Vermont.    

  I  would  like  to  acknowledge  the  members  of  my  PhD  committee,  Dr.  Fiona  Watt,   Dr.   Ángel   Nebreda   and   Dr.   Marisol   Soengas   for   scientific   guidance   and   for   making   possible  all  those  meetings  during  my  PhD.  

  I  want  to  thank  the  collaborators,  Dr.  Peter  Angel,  for  carrying  out  the  microarray   analyses   and   for   scientific   discussion.   Also,   Dr.   Peter   Petzelbauer,   for   sharing   his   knowledge   as   a   dermatophatologist   with   us,   for   travelling   to   Madrid   to   discuss   our   projects  and  for  providing  me  with  so  many  precious  human  samples.      

  I  want  to  thank  the  2008  La  Caixa  fellows.  Matt,  Jarek  S.,  Aga,  Kerstin,  Marta,  Sara,   Miljana,  Jarek  C.,  and  especially  to  Sara  Mainardi,  for  being  such  a  good  friend  inside  and   outside  CNIO,  for  all  those  moments  spent  together  outside  CNIO,  enjoying  the  life  as  it  

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is.   I   also   want   to   thank   Miljana,   for   being   a   great   roomie   and   I   want   to   thank   Marta   Nasila  for  beeing  my  first  friend  in  the  lab.  

  I   would   like   to   thank   many   people   from   CNIO.   Thank   you   Lina,   for   all   those   breakfasts  and  moments  we  spent  together  during  this  time.  I  want  to  thank  Ultan  for   helping  me  with  the  Flow  Cytometer  and  for  all  the  music  you  have  given  to  me  and  for   the   Primavera   Sound   2012!   I   want   to   thank   Carlitos,   for   so   many   concerts   we   went   together.  I  want  to  thank  my  "library  friends"  Laura  and  Bárbara,  for  being  next  to  me   during  this  time  while  I  was  writing  the  thesis  and  for  you  immense  support.  

  Quiero   agradecer   todo   el   apoyo   que   me   dan   mis   amigos,   Cris   Alonso.,   Elena,   Marta,  Bego,  Jesús,  Cristina  Bosch.  Gracias  por  todos  esos  momentos  de  cenas  y  sesiones   de   cine.   Tampoco   quiero   olvidarme   de   mis   amigas   las   biólogas,   repartidas   por   todo   el   mundo.  Asun,  Bea  Buitrago,  Irene  Ureña,  Laura,  Martita,  Ana,  Bea  Cabanillas.  Seguid  así.  

No  dejéis  de  luchar  por  aquello  en  lo  que  creéis.  Gracias  Mª  Luz  por  enseñarme  la  luz  al   final  del  tunel.    

  Lo  más  especial  siempre  llega  al  final.  No  quiero  olvidarme  de  mi  familia.  De  mis   tios,   tias   y   primos,   por   ese   grupo   tan   maravilloso   de   primos   que   siempre   debe   seguir   unido   (¡Viva   Mamblas!).   No   me   quiero   olvidar   de   Tere,   porque   para   mí   has   sido   una   persona  muy  importante  en  mi  vida.  Quiero  agradecerle  a  mi  abuela  Satur  todo  el  amor   que  me  dio  durante  su  vida,  porque  nunca  te  olvidaré  por  muy  lejos  que  te  hayas  ido.  y   porque   me   hubiera   encantando   que   estuvieras   aquí   el   día   de   la   defensa   de   mi   tesis   doctoral.  

  Quiero  agradecer  inmensamente  a  mis  hermanas,  Marta  e  Irene,  porque  sois  las   mejores   hermanas   del   mundo,   las   mejores   amigas   y   porque   me   encanta   compartir   tantos  momentos  juntas  ya  sea  en  la  vida  cotidiana  o  de  viaje.  Porque  me  encanta  hablar   con  vosotras.    

  Por  último  no  tengo  palabras  para  escribir  lo  agradecida  que  estoy  a  mis  padres,     Manuel  y  Feli.  Gracias  por  vuestro  apoyo  incondicional  durante  estos  cuatro  años,  por   vuestro  cariño  y  por  vuestro  inmenso  corazón.    

 

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  T able  of   C ontents

 

       

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TABLE  OF  CONTENTS  

SUMMARY...5  

RESUMEN...9  

ABBREVIATIONS ... 13  

INTRODUCTION... 17  

1.  THE  SKIN ...19  

1.1.  The  Dermis ...19  

1.2.  The  Epidermis ...19  

Figure  I1.... 20  

1.3.  Epidermal  and  dermal  crosstalk ...21  

1.4.  Epidermal  Stem  Cells ...22  

1.5.  Human  skin  versus  mouse  skin...23  

2.  SKIN  CANCER ...23  

2.1.  Basal  Cell  Carcinoma  (BCC)...24  

2.2.  Cutaneous  Squamous  Cell  Carcinoma  (SCC) ...24  

Figure  I2.... 25  

3.  THE  ACTIVATOR  PROTEIN  1  (AP-­‐1)  TRANSCRIPTION  FACTOR ...26  

3.1.    Structure  and  function...26  

Figure  I3.... 26  

3.2.  AP-­1  signal  transduction...27  

Figure  I4.... 27  

3.3.  Biological  functions  of  AP-­1  in  mice...28  

3.3.1.  Biological  functions  of  AP-­‐1  in  skin... 28  

3.3.2.  AP-­‐1  functions  in  tumorigenesis ... 28  

3.3.2.1.  AP-­‐1  functions  in  skin  tumorigenesis... 30  

4.  TUMOR  MICROENVIRONMENT...31  

4.1.  Extracellular  Matrix  (ECM) ...31  

4.2.  Matrix  metalloproteases  (MMPs)...32  

4.3.  Cancer  Associated  Fibroblasts  (CAFs)...33  

4.4.  Inflammation  and  Cancer...34  

4.4.1.  Tumor-­‐protective  inflammation... 34  

4.4.2.  Tumor-­‐promoting  inflammation... 35  

4.4.3.  Skin  inflammation  and  cancer ... 36  

Figure  I5.... 36  

Table  I1.... 38  

OBJECTIVES ... 41  

OBJETIVOS ... 45  

MATERIALS  AND  METHODS... 49  

1.  MICE ...51  

1.1.  Study  approval...51  

1.2.  Generation  of  the  tet-­switchable  c-­fos  allele ...51  

1.3.  Mouse  lines ...51  

1.3.1.  c-­‐FosEp-­‐tetON    and  c-­‐FosEp-­‐tetOFF  mouse  lines... 51  

1.3.2.  c-­‐FosEp-­‐tetON;  Rag1-­‐/-­‐  mouse  line... 52  

1.4.  Mouse  Genotyping...52  

Table  M1.... 52  

1.5.  Mouse  treatments...53  

1.5.1.  Doxycycline  treatment... 53  

1.5.2.  Chemical  carcinogenesis ... 53  

1.5.3.  Anti-­‐inflammatory  treatment ... 53  

1.5.4.  MMP  inhibitory  treatment ... 53  

1.6.  Skin  barrier  assays...53  

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1.6.1.Transepidermal  water  loss  (TEWL)  in  vivo  epidermal  barrier  assay... 53  

1.6.2  Toluidine  Blue  in  vivo  epidermal  barrier  assay... 54  

2.  HISTOLOGICAL  ANALYSIS ...54  

2.1.  Fresh  frozen  tissue ...54  

2.2.  Formalin-­fixed  paraffin-­embedded  tissue ...54  

2.3.  Human  samples  and  Tissue  Microarray  (TMA)  preparation...55  

2.4.  Nile  Red  staining...55  

3.  PROTEIN  ANALYSES...55  

3.1.  Protein  extraction  and  quantification ...55  

3.2.  Immunoblotting...56  

3.3.  Chromatin  Immunoprecipitation  (ChIP) ...56  

4.  RNA  ANALYSES...56  

4.1.  RNA  extraction  from  tissues  or  cells ...56  

4.2.  RNA  extraction  from  FACS-­sorted  cells ...57  

Table  M2.... 57  

Table  M3.... 58  

4.3.  Genome-­wide  expression  analyses...58  

5.  FLOW  CYTOMETRY...59  

5.1.  Back  skin-­specific  protocol...59  

5.2.  Lymph  node-­specific  protocol...60  

5.3.  Flow  cytometry  analyses...60  

5.4.  FACS  sorting...61  

6.  CELL  CULTURE ...61  

6.1.  Keratinocyte  primary  cultures ...61  

6.1.1.Primary  keratinocytes... 61  

6.1.3.  E  Low  Calcium  medium ... 62  

6.1.4.  SCC  cell  lines... 62  

6.1.5.  Feeders ... 62  

6.4.  In  vitro  proliferation  assays...62  

6.4.1.  Cell  Counts... 62  

6.4.2.  Colony  formation  assays ... 62  

6.4.3.  EdU  incoroporation  assay ... 63  

Statistical  analyses...63  

RESULTS ... 65  

1.  INDUCIBLE  EPIDERMAL  C-­FOS  EXPRESSION  IN  ADULT  MICE  LEADS  TO  EPIDERMAL   HYPERPLASIA  WITH  INCREASED  PROLIFERATION ...67  

1.1.  Inducible  keratinocyte-­specific  c-­fos  expression:  c-­FosEp-­tetON  mouse  model...67  

Figure  1... 67  

Figure  2... 69  

1.1.2.  c-­Fos  promotes  proliferation  in  vivo  in  a  non-­cell  autonomous  manner...70  

Figure  3... 70  

Figure  4... 71  

1.1.3.  Impaired  differentiation  upon  c-­fos  expression  in  vitro ...72  

Figure  5... 73  

1.2.  Inducible  keratinocyte-­specific  c-­fos  expression:  c-­FosEp-­tetOFF  mouse  model...74  

Figure  6... 74  

Figure  7... 75  

1.2.1.  The  epidermal  barrier  is  not  affected  upon  c-­fos  expression ...76  

Figure  8... 77  

2.  MMP10  AND  S100A7A15  ARE  TWO  NOVEL  TRANSCRIPTIONAL  TARGET  GENES  OF  C-­‐FOS....78  

2.1.  Genome-­wide  expression  analyses  revealed  novel  target  genes  of  c-­Fos  in  keratinocytes .78   2.2.Validation  of  c-­Fos  target  genes  in  vitro...78  

Figure  9... 79  

2.3.  Validation  of  c-­Fos  target  genes  in  vivo ...79  

Figure  10.... 80  

2.4.  Mmp10  and  s100a7a15  promoter  analyses ...81  

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Figure  11.... 81  

3.  CFOS  EXPRESSION  INDUCES  SKIN  INFLAMMATION  CHARACTERIZED  BY  CHRONIC  CD4  T   CELL  RECRUITMENT ...82  

Figure  12.... 83  

Figure  13.... 84  

Figure  14.... 85  

4.  INTERFERING  WITH  CD4  T  CELL  RECRUITMENT  SIGNIFICANTLY  IMPAIRS  C-­‐FOS-­‐ MEDIATED  EPIDERMAL  HYPERPLASIA...86  

Figure  15.... 87  

5.  BROAD  MMP  INHIBITION  PREVENTS  THE  DEVELOPMENT  OF  PRENEOPLASTIC  LESIONS   UPON  C-­‐FOS  EXPRESSION  IN  C-­‐FOSEPTETON  MICE ...88  

Experimental  set-­‐up.    Control  and  c-­‐FosEp-­‐tetON  mice  were  treated  with  Dox  and  with  vehicle  or  10mg/kg  of   TAPI-­‐1  injected  IP  three  times  a  week  for  4  weeks... 88  

Figure  17.... 89  

6.  C-­‐FOS-­‐DEPENDENT  SKIN  PHENOTYPE  IS  LARGELY  REVERSIBLE ...90  

Figure  18.... 91  

Figure  19.... 92  

7.  DMBA-­‐INDUCED  PAPILLOMA  AND  SCC  DEVELOPMENT  IS  ACCELERATED  BY  C-­‐FOS...93  

7.1.  c-­FosEp-­tetON  mice  develop  invasive  SCCs  upon  DMBA...93  

Figure  20.... 94  

Figure  21.... 95  

Figure  22.... 96  

7.2.  c-­FosEp-­tetOFF  mice  develop  highly  invasive  SCCs  upon  DMBA ...97  

Figure  23.... 97  

Figure  24.... 98  

7.3.  Impaired  mmp10  and  s100a7a15  expression  in  c-­fos  deficient  K5-­SOS+  tumor-­prone  mice ...98  

Figure  25.... 99  

7.4.  Sulindac  treatment  reduces  SCC  size  and  number...99  

Figure  26.... 100  

8.  HUMAN  SCCS  EXPRESS  HIGH  C-­‐FOS  PROTEIN  LEVELS  CORRELATING  WITH  HIGH  MMP10   BUT  NOT  WITH  S100A7  EXPRESSION  LEVELS ... 101  

Figure  27.... 102  

8.1.  SCCs  but  not  BCCs  express  c-­Fos  and  this  correlates  with  MMP10  expression...102  

Figure  28.... 103  

Figure  29.... 104  

8.2.  c-­FOS  protein-­expressing  SCCs  present  CD4  T  lymphocyte  infiltrates...104  

Figure  30.... 105  

DISCUSSION ...107  

1.  C-­‐FOS  IN  EPIDERMAL  HOMEOSTASIS... 109  

2.  C-­‐FOS  TRIGGERS  INFLAMMATORY  PROCESSES  IN  THE  SKIN  THAT  LEAD  TO  THE   DEVELOPMENT  OF  PRENEOPLASTIC  LESIONS... 111  

3.  C-­‐FOS  TRANSCRIPTIONALLY  CONTROLS  MMP10  AND  S100A7A15  EXPRESSION ... 115  

4.  C-­‐FOS  FUNCTIONS  IN  SKIN  CANCER  DEVELOPMENT  AND  PROGRESSION ... 117  

Figure  31.... 121  

CONCLUSIONS ...123  

CONCLUSIONES...129  

REFERENCES...135  

APPENDIX...151  

Table  A... 153    

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S ummary  

 

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In   this   study   I   describe   a   novel   mechanism   by   which   increased   levels   of   c-­‐

Fos/AP-­‐1  transcription  factor  in  the  epidermis  promotes  the  development  of  epidermal   preneoplastic   lesions   and   eventually,   upon   7,12-­‐dimethyl-­‐benz[a]anthracene   (DMBA)   treatment,  it  contributes  to  the  development  of  skin  Squamous  Cell  Carcinomas  (SCCs).  

To  unravel  the  function  of  epidermal  c-­‐Fos,  we  have  generated  a  mouse  model  (c-­‐FosEp-­

tetON)  in  which  we  can  inducibly  activate  the  expression  of  c-­fos  in  the  basal  layer  of  the   epidermis  as  well  as  in  other  stratified  epithelia.  I  show  that  inducible  c-­fos  expression   triggers  innate  and  adaptive  immune  responses  in  the  epidermis,  particularly,  transient   recruitment   of   Gr1+   cells   and   chronic   recruitment   of   CD4   T   lymphocytes.   In   addition,   broad  genome-­‐wide  expression  analyses  identified  two  direct  and  novel  transcriptional   target   genes   of   c-­‐Fos,   mmp10   and   s100a7a15.   Both   target   genes   are   involved   in   inflammatory  processes,  being  able  to  recruit  Gr1+  cells  and  CD4  T  lymphocytes,  as  well   as   in   the   development   of   cutaneous   cancers.   Importantly,   using   a   broad   matrix   metalloprotease   (MMP)   inhibitor   to   reduce   MMP10   activity   in   the   epidermis,   we   observed   amelioration   of   the   development   of   the   preneoplastic   lesions   of   the   skin.    

Furthermore,  in  the  absence  of  mature  B  and  T  cells  in  a  Rag1-­‐deficient  background,  a   drastic   improvement   of   the   disease   in   FosEp-­tetON   mice   was   observed.   Moreover,   upon   DMBA-­‐induced  H-­‐Ras  mutations,  c-­‐Fos  is  sufficient  to  promote  the  development  of  skin   SCCs.   Interstingly,   in   this   setting,   tumor   size,   number   and   burden   were   significantly   reduced  upon  blockade  of  inflammatory  responses  by  means  of  a  cyclooxygenase  1  and   2   (COX-­‐1/COX-­‐2)   inhibitory   treatment   following   DMBA   treatment   and   inducible   expression  of  c-­fos.  Finally,  I  have  seen  a  strong  correlation  between  human  c-­‐FOS  and   MMP10  expression  in  human  SCCs,  where  they  are  abundantly  expressed,  compared  to   BCCs,   where   no   expression   of   these   two   proteins   is   observed.   In   addition,   a   strong   correlation  between  c-­‐FOS  expression  and  CD4  T  cell  infiltrates  were  observed  in  human   SCCs.   This   thesis   has   identified   two   novel   and   direct   transcriptional   targets   of   c-­‐Fos,   MMP10   and   S100a7a15,   clearly   involved   in   mediating   CD4   T   cell-­‐mediated   immune   responses   in   the   epidermis   and   thereby   contributing   to   the   development   of   preneoplastic  lesions,  which  upon  oncogenic  insults,  eventually  develop  into  SCCs.  Here   I  propose  two  new  candidate  proteins  that  could  be  of  therapeutic  interest  to  treating   cutaneous  SCCs.  

 

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R esumen  

   

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  Los   resultados   de   mi   proyecto   de   tesis   han   dado   lugar   a   la   descripción   de   un   nuevo   mecanismo   mediante   el   cual   el   factor   de   transcripción   c-­‐Fos/AP-­‐1   promueve   el   desarrollo  de  lesiones  preneoplásicas  en  la  epidermis  y  en  combinación  con  la  aplicación   de  DMBA,  promueve  el  desarrollo  de  carcinomas  epidermoides  (SCCs).  Para  estudiar  la   función  de  c-­‐Fos  en  la  epidermis,  hemos  generado  un  modelo  genético  de  ratón  (c-­‐FosEp-­

tetON)  en  el  cual  se  puede  inducir  la  expresión  de  c-­fos  en  la  capa  basal  de  la  epidermis  y   en   otros   epitelios   estratificados.   Aquí   demuestro   que   la   expresión   inducible   de   c-­fos   promueve  respuestas  inmunes  innatas  y  también  adaptativas  en  la  piel,  fomentando  la   infiltración   de   células   Gr1+   transitoriamente   y   de   linfocitos   T   CD4+   de   forma   crónica.  

Mediante   análisis   de   expresión   genómica   se   identificaron   dos   nuevos   genes   diana,   mmp10  y  s100a7a15,  ambos  implicados  en  procesos  inflamatorios  así  como  también  en   cánceres   de   piel.   La   inhibición   de   metalloproteasas   (MMPs)   mediante   el   uso   de   un   inhibidor,  redujo  significativamente  la  progresión  de  las  lesiones  preneoplásicas  tras  la   inducción  de  la  expresión  de  c-­fos  en  ratones  c-­‐FosEp-­tetON.  Además,  una  mejora  drástica   se   observó   en   el   80%   de   los   casos   al   deplecionar   las   poblaciones   de   linfocitos   T   y   B   maduros,  mediante  el  uso  de  un  ratón  knock-­‐out  para  Rag1.  Asimismo,  en  esta  tesis  he   demostrado   que   el   factor   de   transcripción   c-­‐Fos/AP-­‐1   es   suficiente   para   promover   el   desarrollo  de  carcinomas  epidermoides  en  ratones  tratados  con  el  carcinógeno  DMBA.  

En   este   mismo   sistema,   el   bloqueo   de   procesos   inflamatorios   en   la   piel,   mediante   la   inhibición   de   las   enzimas   COX1   y   COX2,   en   ratones   inducidos   con   DMBA   y   c-­‐Fos   se   observa   una   disminución   en   el   desarrollo   de   carcinomas   epidermoides   y   aquellos   desarrollados   son   más   pequeños.   Finalmente,   los   análisis   de   muestras   humanas   de   carcinomas   epidermoides   y   carcinomas   basales   de   piel   han   descubierto   la   posible   implicación   de   c-­‐FOS   sólo   en   los   carcinomas   epidermoides   dado   que   el   80%   de   estos   tumores  presentaba  altos  niveles  de  c-­‐FOS,  mientras  que  los  carcinomas  basales  no  lo   expresaban.  Finalmente,  he  observado  una  correlación  entre  la  expresion  de  c-­‐FOS  y  de   MMP10  en  carcinomas  epidermoides,  MMP10  podría  perfectamente  ser  un  gen  diana  de   c-­‐FOS  en  humano  como  observamos  en  ratón.  Asimismo,  se  observó  correlación  entre   los  niveles  de  expresión  de  c-­‐FOS  en  los  carcinomas  epidermoides  y  los  altos  niveles  de   infiltración   de   células   T   CD4+.   Esta   tesis   ha   servido   para   identificar   dos   genes   transcripcionalmente  activados  por  c-­‐Fos,  mmp10  y  s100a7a15,  claramente  implicados   en  el  desarrollo  de  procesos  inflamatorios  mediados  por  células  T  CD4+  en  la  piel  y  que  

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promueven   inicialmente   el   desarrollo   de   lesiones   preneoplásicas   y   eventualmente   el   desarrollo   de   carcinomas   epidermoides.     El   desarrollo   de   fármacos   específicos   para   estas  dos  dianas  puede  ser  de  uso  terapéutico  en  carcinomas  epidermoides.    

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A bbreviations  

 

 

   

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ABBREVIATIONS  

ADAM   A  disintegrin  and  metalloproteinase  

ADAMTS     A  disintegrin  and  metallopreinase  with  thrombospoindin  motifs   AP-­‐1   Activator  Protein  1  

ATF   Activating  transcription  factor   BCC   Basal  Cell  Carcinoma  

BSA   Bovine  Serum  Albumine   ChIP   Chromatin  IP  

CTLS   Cytotoxic  T  lymphocytes   DC   Dendritic  cell  

DMBA   7,12-­‐dimethyl-­‐benz[a]anthracene    

Dox   Doxycycline  

ECM   Extracellular  matrix   EdU   5-­‐ethynyl-­‐2`-­‐deoxyuridine   EGF   Epidermal  growth  factor  

EGFR   Epidermal  growth  factor  receptor   ERK   Extracellular  signal  regulated  kinase   FBS   Fetal  bovine  serum  

GM-­‐CSF   Granulocyte  monocyte  colony  stimulating  factor   HEK   Human  epidermal  keratinocytes  

HF   Hair  follicle  

HPV   Human  papillomavirus  

IBD   Inflammatory  bowel  disease   IEL   Intraepithelial  lymphocyte   IFE   Interfollicular  epidermis  

IHC   Immunohistochemistry  

IP   Intraperitoneal  

JNK   Jun  N-­‐terminal  kinase  

K1   Keratin  1  

K10   Keratin  10  

K5   Keratin5  

K6   Keratin  6  

KGF   Keratinocyte  growth  factor   LOH   Loss  of  heterozigosity   LOX   Lysil  oxidase  

MAPK   Mitogen-­‐activated  protein  kinase  

MMP   Matrix  Metalloprotease  

NK   Natural  Killer  

NMSC   Non  melanoma  skin  cancer   OCT   Optimal  cutting  temperature   PBS   Phosphate  buffered  saline  

PDAC   Pancreatic  ductal  adenocarcinoma  

PTCH1   Patched1  

RT   Room  temperature  

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RtTA   Reverse  transactivator  

SC   Stem  cell  

SCC   Squamous  Cell  Carcinoma   SDS   Sodium  dodecyl  sulfate  

SHH   Sonic  Hedgehog  

SLE   Systemic  Lupus  Erythematosus  

SMO   Smoothened  

SOS   Son  of  Seveless  

TACE   TNFa-­‐Converting  Enzyme  

Tet   Tetracycline  

TEWL   Transepidermal  Water  Loss   Tgf-­‐β   Transforming  Growth  Factor  Beta   TNFα   Tumor  necrosis  factor  alpha  

TPA   12-­‐O-­‐Tetradecanoylphorbol-­‐13-­‐acetate    

tTA   Transactivator  

VEGF   Vascular  endothelial  growth  factor  

 

 

 

 

 

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I ntroduction  

 

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1.  THE  SKIN    

The  skin  is  the  body´s  largest  organ.  It  serves  as  a  protective  barrier  that  protects   against   loss   of   fluids,   physical   trauma   and   invasion   by   harmful   microbes.   The   skin   is   divided   into   two   different   compartments,   the   dermis   and   the   epidermis.   Interactions   between  epithelial  and  mesenchymal  cells  play  a  crucial  role  in  the  regulation  of  tissue   morphogenesis,  homeostasis  and  repair  (Beck  and  Blanpain,  2012).  

1.1.  The  Dermis  

The   dermis   is   the   fibrous   connective   tissue   between   the   epidermis   and   the   subcutaneous  fat  and  is  responsible  for  providing  nutrients  and  physical  support  to  the   epidermis   (Burr   and   Penzer,   2005).   The   most   abundant   cell   type   in   the   dermis   is   the   fibroblast  (McLafferty  et  al.,  2012).  Fibroblasts  synthesize  the  extracellular  matrix  and   collagen  required  for  normal  homeostasis.  Type  I  collagen  is  by  far  the  most  abundant   protein  in  human  skin,  comprising  greater  than  90%  of  its  dry  weight  and  the  unique   physical  properties  of  collagen  fibers  is  to  confer  structural  integrity  to  skin  (Fisher  et   al.,   2008).     The   dermis   also   contains   blood   and   lymph   vessels,   nerve   endings,   hair   follicles   and   glands.   Immune   cells   also   populate   the   dermis.   Some   immune   cells   like   mastocytes,   histiocytes   and   γ/δ   T   lymphocytes   are   resident   in   the   skin,   but   other   leukocytes   like   T   cells   migrate   to   the   skin   upon   injury   or   infection   (Gebhardt   et   al.,   2011).  

1.2.  The  Epidermis  

The  epidermis  is  a  stratified  epithelium  that  contains  a  single  inner  (basal)  layer   of  proliferative  keratinocytes  that  adhere  to  the  basement  membrane,  which  is  rich  in   extracellular   matrix   and   growth   factors,   and   separates   the   epidermis   from   the   underlying  dermis.  Cells  in  the  basal  layer  are  responsible  for  generating  the  layers  of   non-­‐dividing   cells   that   undergo   a   program   of   terminal   differentiation   as   they   move   outward  and  are  continually  shed  from  the  skin  surface  (Figure  1)  (Fuchs  and  Nowak,   2008).  The  balance  between  proliferation  and  differentiation  is  tightly  regulated,  since   the   disruption   of   this   balance   causes   several   pathological   conditions   including   inflammation  and  tumorigenesis  (Blanpain  and  Fuchs,  2009).  Indeed,  a  disruption  of  the   differentiation-­‐promoting   Notch   signaling   pathway   or   a   hyperactivation   of   the   EGFR-­‐

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Ras-­‐MAPK   signaling   pathway   in   keratinocytes,   leads   to   the   development   of   epithelial   tumors  (Demehri  et  al.,  2009;  Brown  et  al.,  1998).  

Figure  I1.    

                     

The skin and its appendages. Cross-section through mammalian skin and a hair follicle (Fuchs and Raghavan, 2002)  

As   epidermal   keratinocytes   exit   the   basal   layer   and   cease   to   proliferate,   they   progress   upward   through   three   distinct   differentiation   stages:   spinous   layer,   granular   layer   and   stratum   corneum.   The   major   structural   change   at   the   basal-­‐to-­‐spinous-­‐layer   transition  is  the  switch  from  keratin  5  and  keratin  14  intermediate  filaments  in  the  basal   layer   to   Keratin   1   and   Keratin   10   suprabasally.   Additional   changes   occur   in   the   basal/spinous  transition,  such  as  downregulation  of  p63,  a  member  of  the  p53  family  of   transcription   factors   (Dotto,   2009).   p63   is   expressed   in   basal   cells   of   all   stratified   epithelia   and   is   thought   to   represent   a   master   regulator   of   the   stratification   process   (Blanpain   et   al.,   2007).   Indeed,   p63-­‐deficient   mice   die   postnatally   from   severe   developmental  anomalies,  including  a  lack  of  stratified  epithelia  (Mills  et  al.,  1999).    

As  cells  enter  the  granular  layer,  the  primary  cornified  envelope  protein  loricrin   is   expressed   and   lamellar   granules   packed   full   of   lipids   appear   (Blanpain   and   Fuchs,   2009).   Profilaggrin   is   also   expressed   at   this   time,   and   soon   afterwards,   it   is   proteolytically  processed  to  generate  filaggrin,  a  protein  that  bundles  keratin  filaments  

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into   indestructible   cables   (Aho   et   al.,   2012).   As   granular   cells   transit   to   the   stratum   corneum,  the  metabolical  activity  ceases,  and  an  influx  of  calcium  results  in  activation  of   transglutaminases,   that   initiate   glutamyl-­‐e-­‐lysine   crosslinks   to   produce   the   cornified   envelope,   characteristic   of   this   layer   (Eckert   et   al.,   2005).   The   cornified   envelope   surrounds   cells   in   the   stratum   corneum   and   contributes   to   the   skin's   barrier   function   (Simpson   et   al.,   2011).     Eventually,   keratinocytes   in   the   stratum   corneum   undergo   apoptosis   and   are   released   from   the   surface   of   the   epidermis   (Blanpain   and   Fuchs,   2009).  

The  epidermis  also  has  the  remarkable  ability  to  elaborate  the  body  surface  with   appendages,  which  range  from  hair  follicles,  nails,  oil  and  sweat  glands  in  mammals  to   scales  and  feather  in  lower  vertebrates  (Fuchs  and  Nowak,  2008).    

Besides   keratinocytes,   three   other   cell   types   are   found   in   the   epidermis:  

melanocytes,   Langerhans   cells   and   Merkel   cells.   They   are   not   abundant,   but   have   important  functions.  Melanocytes  are  located  in  the  lower  part  of  the  epidermis  and  they   synthesize   melanin,   the   pigment   that   gives   skin   the   natural   color   (Haass   and   Herlyn,   2005).   Langerhans   cells   are   dendritic   cells   (antigen-­‐presenting   immune   cells)   of   the   epidermis  and  they  are  present  in  all  layers  of  the  epidermis,  but  are  most  prominent  in   the  stratum  spinosum  where  they  take  up  and  process  microbial  antigens  to  become  fully   functional  antigen  presenting  cells  (Romani  et  al.,  2012).  Merkel  cells  are  oval  receptor   cells   that   have   synaptic   contacts   with   somatosensory   neurons   and   these   cells   are   involved  in  the  sensation  of  light  touch  (Boulais  and  Misery,  2007).  

1.3.  Epidermal  and  dermal  crosstalk  

Interactions   between   mesenchymal   and   epithelial   cells   are   responsible   for   complex  events  such  as  tissue  development,  homeostasis  and  repair  (Werner  and  Smola,   2001).  This  mutual  crosstalk  mainly  involves  growth  factors  and  cytokines.    Pioneering   studies   of   Rheinwald   and   Green   demonstrated   that   normal   human   epidermal   keratinocytes  depend  on  the  presence  of  fibroblasts  for  efficient  growth  in  tissue  culture   (Rheinwald   and   Green,   1975).   Later   on   Rubin,   et   al   identified   a   fibroblast-­‐derived   growth  factor  (FGF),  termed  Keratinocyte  Growth  Factor  (KGF),  that  strongly  stimulated   the   proliferation   of   keratinocytes   (Rubin   et   al.,   1989).   Moreover,   the   group   of   Peter   Angel   described   a   paracrine   loop   in   which   by   using   immortalized   fibroblasts   deficient  

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for   c-­‐Jun   and   JunB,   in   combination   with   human   primary   keratinocytes   in   the   three-­‐

dimensional  organotypic  co-­‐culture  system,  observed  that  the  lack  of  either  one  of  these   transcription  factors  in  fibroblasts  severely  affected  proliferation  and  differentiation  of   the  overlying  normal  human  keratinocytes  (Szabowski  et  al.,  2000).  This  was  due  to  a   direct  transcriptional  regulation  of  KGF  and  GM-­‐CSF  by  Jun/AP-­‐1  proteins  in  fibroblasts.  

Furthermore,   this   crosstalk   could   also   have   an   impact   in   epithelial   tumorigenesis.  

Indeed,  recent  studies  have  shown  that  a  disruption  in  the  Notch  signaling  pathway  in   the   mesenchymal   compartment   leads   to   the   secretion   of   soluble   factors   in   an   AP-­‐1   dependent   manner   (FGF7,   FGF10,   CSF1,   MMP3   and   MMP13).   These   factors   create   an   appropriate  microenvironment  in  the  dermis,  also  termed  as  "field  cancerization",  that   promotes  epithelial  tumorigenesis  (Hu  et  al.,  2012).  

1.4.  Epidermal  Stem  Cells  

  The   adult   epidermis   and   its   appendages   undergo   continuous   renewal   and   maintain  reservoirs  of  multipotent  stem  cells  (SC).  Different  stem  cell  pools  have  been   found  in  the  hair  follicle  (HF)  as  well  as  in  the  interfollicular  epidermis  (IFE).    

  HF   stem   cells   reside   in   a   specialized   microenvironment   called   the   bulge.   These   cells   cycle   slowly,   as   revealed   by   their   ability   to   retain   a   pulse   of   nucleotide   label   following   weeks   of   chase   (Alonso   and   Fuchs,   2003).   The   bulge   is   composed   of   a   heterogeneous  population  of  self-­‐renewing  multipotent  cells.  Stem  cell  subpopulations   in   the   bulge   exhibit   different   locations   (basal   versus   suprabasal)   and   different   characteristics,   like   slowly   cycling   (quiescent)   versus   rapidly   cycling   (Fuchs,   2009).   In   contrast   to   the   HF,   much   less   is   known   about   stem   cells   in   the   IFE.   Although   lineage-­‐

tracing  experiments  have  clearly  demonstrated  that  homeostasis  in  mouse  epidermis  is   fueled   by   an   independent   stem   cell   population,   their   origin   and   localization   is   still   a   matter  of  debate  (Beck  and  Blanpain,  2012).  

Stem   cells   in   the   basal   layer   of   the   epidermis   can   undergo   symmetric   and   asymmetric   cell   division.   The   maintenance   of   a   constant   pool   of   stem   cells   can   be   accomplished  by  one  of  two  distinct  types  of  cell  divisions  during  tissue  homeostasis:  in   asymmetric  division,  where  one  daughter  remains  a  SC  throughout  self-­‐renewal,  and  the   other   daughter   becomes   committed   to   enter   a   program   of   terminal   differentiation.   By  

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which   for   SCs   would   result   in   the   generation   of   two   SCs   (self-­‐renewal)   or   two   differentiated  cells  (symmetric  differentiation).      

1.5.  Human  skin  versus  mouse  skin  

 The   stratification   of   mouse   skin   and   human   skin   is   similar—although   distinct   differences  do  exist,  such  as  the  increased  thickness  of  human  skin  in  comparison  with   that   of   mice   (Lowes   et   al.,   2007).   Mouse   skin   is   heavily   populated   by   hair   follicles,   whereas  the  human  epidermis  is  mainly  interfollicular;  the  differences  are  less  striking   in  skin  from  the  ear  and  the  tail  of  mice  compared  with  the  hairy  back  skin.  Moreover,   mouse  skin  lacks  sweat  glands  and  melanocytes  in  the  interfollicular  epidermis,  but  in   contrast  shows  a  synchronized  hair  cycle,  rapid  epidermal  turnover  and  the  presence  of   intra   epidermal   γδ   T   cells   (Berking   et   al.,   2002;   Jameson   et   al.,   2004;   Khavari,   2006;  

Wagner  et  al.,  2010).  The  murine  immune  system  contains  particular  subtypes  of  cells,   including  CD8+  dendritic  cells  (DCs),  dendritic  epidermal  T  cells  and  natural  killer  (NK)   1.1+   T   cells   that   are   absent   in   human   skin.   Despite   the   obvious   differences   between   mouse  skin  and  human  skin,  mouse  models  have  been  successfully  employed  to  mimic   human  skin  disease  in  contact  hypersensitivity,  wound  healing,  inflammation  as  well  as   skin   cancer   to   model   monogenic   hereditary   skin   diseases.   Clearly,   mouse   and   human   skin  have  many  aspects  and  molecular  pathways  in  common.    

2.  SKIN  CANCER    

Skin  cancer  is  the  third  most  common  human  malignancy  and  its  occurrence  has   been  increasing  rapidly  over  the  past  decades.  An  estimated  number  of  2-­‐3  million  non-­‐

melanoma   skin   cancer   patients   and   132,000   patients   of   melanoma   are   counted   every   year  (World  Health  Organization).  

Melanoma  is  the  type  of  skin  cancer  that  arises  from  the  melanocytes,  melanin-­‐

producing  cells  located  in  the  basal  layer  of  the  epidermis.  It  is  the  most  dangerous  type   of  skin  cancer  as  it  is  the  leading  cause  of  death  from  skin  disease  (Tsao  et  al.,  2012).    

10%  of  melanoma  patients  have  a  family  history  that  confers  approximately  a  twofold   increase   in   probability   to   develop   melanoma.   Several   genes   have   been   identified   to   predispose  to  melanoma.  Amongst  others,  mutations  in  CDKN2A  (encoding  p16),  CDK4,  

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RB1   lead   to   the   development   of   melanoma.   Other   genes   such   as   PTEN   or   B-­‐RAF   have   been  described  to  promote  melanoma  (Maubec  et  al.,  2012;  Rezze  et  al.,  2012).  

Non-­‐Melanoma  Skin  cancer  comprises  two  major  types  of  Skin  Cancers,  Basal  and   Squamous  Cell  Carcinoma  (BCC  and  SCC).  Both  tumors  arise  from  keratinocytes,  but  are   very  different  in  morphology  and  in  the  underlying  mechanisms  (Colmont  et  al.,  2012).      

2.1.  Basal  Cell  Carcinoma  (BCC)  

It   is   the   most   common   and   least   dangerous   form   of   skin   cancer   (Kasper   et   al.,   2012).  It  grows  slowly,  usually  on  the  head,  neck  and  upper  torso.  BCCs  appear  on  skin   exposed  to  UV  light  radiation  and  typically  occur  in  the  fourth  decade  of  life  and  beyond   (Kasper  et  al.,  2012).  Pathologically,  it  resembles  the  keratinocytes  in  the  basal  layer  of   the   epidermis   (Crowson,   2006).   The   vast   majority   of   BCCs   occur   sporadically,   but   patients   with   the   rare   heritable   disorder   “Basal   cell   nevus   syndrome”   have   a   marked   susceptibility  to  developing  BCCs.  Several  genes  of  the  Sonic  Hedgehog  (SHH)  signaling   pathway  are  frequently  mutated  (Epstein,  2008).  Approximately  90%  of  sporadic  BCCs   have  identifiable  mutations  in  at  least  one  allele  of  PTCH1,  and  an  additional  10%  have   activating   mutations   in   the   downstream   effector,   smoothened   (SMO)   protein,   which   renders   SMO   resistant   to   inhibition   by   PTCH1   (Epstein,   2008).     Several   compounds   targeting  members  of  the  SHH  signaling  pathway  are  being  used  in  clinical  trials  (Kasper   et   al.,   2012).   Removal   of   tumors   using   surgery   is   widely   established   in   less   invasive   BCCs.    

2.2.  Cutaneous  Squamous  Cell  Carcinoma  (SCC)  

Cutaneous  Squamous  cell  carcinoma  is  the  second  most  common  type  of  human   cancer  with  over  250,000  new  cases  annually  in  the  USA  and  it  is  the  second  in  incidence   after  BCC.  It  arises  from  keratinocytes  of  the  epidermis  and  oral  mucosa.  Pathologically,   keratinocytes  in  this  type  of  cancer  share  features  with  the  squamous  cells  seen  in  the   outermost   layers   of   the   epidermis.   Unlike   BCCs,   cutaneous   SCCs   are   associated   with   a   substantial   risk   of   metastasis   (Ratushny   et   al.,   2012).   SCC   is   most   commonly   found   in   sun-­‐exposed  areas.  Besides  ultraviolet  light,  other  risk  factors  have  been  associated  with   skin   SCC,   such   as   arsenic   exposure,   tobacco   and   human   papilloma   virus   infection   (Brantsch  et  al.,  2008).  SCC  typically  manifests  as  a  spectrum  of  progressively  advanced  

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malignancies,   ranging   from   a   precursor   lesion   like   actinic   keratosis   to   SCC   "in   situ",   invasive  SCC  and  finally  metastatic  SCC  (Figure  4)  (Ratushny  et  al.,  2012).    

Figure  I2.  

         

Histological   features   of   the   different   stages   of   human   SCC   development,   from   healthy   skin   to   metastatic  SCC.  

  Several  syndromes  like  Xeroderma  Pigmentosum  or  Epidermolysis  bullosa  have   been  associated  with  increased  risk  to  develop  SCCs.  As  with  other  cancers,  SCCs  exhibit   impaired   genomic   maintenance   that   facilitates   acquisition   of   new   mutations.   p53   is   commonly   mutated   in   dysplastic   lesions.   40%   of   SCC   in   situ   harbors   p53   mutations,   indicating   that   p53   loss   occurrs   prior   to   tumor   invasion   (Campbell   et   al.,   1993).    

Aberrant  activation  of  EGFR  (Epidermal  Growth  Factor)  and  Fyn,  a  Src-­‐family  tyrosine   kinase,  are  seen  in  human  SCCs.  Furthermore,  amplification  and  activating  mutations  of   the  Ras  oncogene  have  been  found  in  SCCs  (Pierceall  et  al.,  1991).  21%  of  SCCs  harbor   activating  Ras  mutations.  Of  the  three  Ras  genes,  Harvey  rat  sarcoma  virus  oncogene  (H-­

Ras)  is  preferentially  mutated  in  SCCs.      

Skin   SCC   has   been   extensively   modeled   by   either   making   use   of   genetically   modified  mice,  such  as  K14-­‐HPV  or  the  K5-­‐SOS  mouse  models  (Arbeit  et  al.,  1994;  Sibilia   et  al.,  2000),  or  by  using  the  two-­‐step  chemical  carcinogenesis  protocol  (Kemp,  2005).  In   this  protocol,  mutations  in  H-­Ras  are  induced  by  a  single  topical  dose  of  a  carcinogen,   most   commonly   7,12-­‐dimethyl-­‐benz[a]anthracene   (DMBA),   applied   on   the   back   skin.  

Repeated   topical   applications   of   a   tumor   promoter,   such   as   TPA   give   rise   to   benign   neoplastic  lesions,  which  causes  sustained  hyperplasia  (papillomas)  and  inflammation.  

A   small   percentage   of   these   papillomas   progress   to   malignant   invasive   squamous   cell   carcinomas   (SCC).   In   carcinomas,   loss   of   heterozygosity   (LOH)   and   mutations   of   the   tumor  suppressor  p53  are  frequent.  More  aggressive  carcinomas  show  additional  LOH   and  mutations  of  the  tumor  suppressors  p19/Arf  and  p16Ink4a  (Kemp,  2005).  The  use  of  

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