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Method Development and Validation

Method development and validation for the determination of cabergoline in tablets by capillary zone electrophoresis

Method development and validation for the determination of cabergoline in tablets by capillary zone electrophoresis

... (CZE) method has been developed for the analysis of caber- goline in its pharmaceutical ...kV and hydrodynamic injection for 4 s. Cabergoline and internal standard verapamil were detected at a ...

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Development and validation of a RP HPLC method for the quantifi

Development and validation of a RP HPLC method for the quantifi

... rapid and sensitive reversed phase high performance liquid chromatographic method has been developed for quantitative analysis of sparfloxacin in pharmaceutical ...The method was validated according ...

7

Development and validation of a liquid chromatography isotope dilution mass spectrometry method for the reliable quantificationof alkylphenols in environmental water samples by isotopepattern deconvolution

Development and validation of a liquid chromatography isotope dilution mass spectrometry method for the reliable quantificationof alkylphenols in environmental water samples by isotopepattern deconvolution

... 4 peaks from the analyte. On the other hand, in LC-MS/MS the overall NP isomers elute as a single chromatographic peak associated to transition 219 > 133. This transition suggests that the α-carbon of the nonylphenols ...

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Development and validation of a capillary electrophoresis method for direct measurement of isocitric, citric, tartaric and malic acids as adulteration markers in orange juices / L  Saavedra, A  García and C  Barbas

Development and validation of a capillary electrophoresis method for direct measurement of isocitric, citric, tartaric and malic acids as adulteration markers in orange juices / L Saavedra, A García and C Barbas

... Capillary electrophoresis (CE) has proved to be a MO, USA). Phosphoric acid 85% was from Merck good choice for investigation of samples in aqueous (Darmstadt, Germany), sodium hydroxide from Pan- media, since usually no ...

8

Development and validation of the Overall Personality Assessment Scale (OPERAS)

Development and validation of the Overall Personality Assessment Scale (OPERAS)

... desirability and acquiescence effects to be obtained. Method: Scales were created using recently developed methods to control response bias effects in a sample of 3,838 participants from a wide age ...

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Development and validation of a scale to identify attitudes towards disability in higher education

Development and validation of a scale to identify attitudes towards disability in higher education

... universities, and there are no tools that specifi cally measure this construct within a university ...context. Method: The design and validation of the CUNIDIS (‘Questions about University ...

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Development and validation of spectrophotometric and ion pair chromatographic techniques for estimation of telmisartan and hydrochlorothiazide

Development and validation of spectrophotometric and ion pair chromatographic techniques for estimation of telmisartan and hydrochlorothiazide

... chromatographic method was developed for estimation of TEL and HYD which can be conveniently employed for routine quality control in pharmaceutical dosage ...times and poor ...telmisartan and ...

10

Development and validation of a BEAMnrc component module for a miniature multileaf collimator

Development and validation of a BEAMnrc component module for a miniature multileaf collimator

... The development was performed using a modified EGSnrc platform which enables us to work in the Microsoft Visual Studio ...modelled. Validation was performed by two methods: (a) a ray-tracing method ...

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Development and validation of numerical modeling approaches for triaxially braided composites

Development and validation of numerical modeling approaches for triaxially braided composites

... elastic and nonlinear behaviour of textile and braided ...damage development and failure of textile ...yarn and matrix pockets is imported into a finite element commercial-code, meshed ...

222

Development and validation of the family motivational climate questionnaire (FMC-Q)

Development and validation of the family motivational climate questionnaire (FMC-Q)

... develop and validate the Family Motivational Climate Questionnaire ...FMCQ. Method: 570 Secondary-School students formed the ...analysis and correlation and regression analyses were ...

9

Development and validation of a capillary electrophoresis method for short chain organic acids measurement in natural rubber latex / V  Galli, N  Olmo and C  Barbas

Development and validation of a capillary electrophoresis method for short chain organic acids measurement in natural rubber latex / V Galli, N Olmo and C Barbas

... imported and were representa- 14 organic acids with indirect UV detection using a tive of commercial ...snow and rain water and Shirao et gation has been utilised, but it needs 30 000 rpm for ...

11

Development and validation of stability indicating RP-HPLC method for the determination of ezetimibe in pharmaceutical dosage forms

Development and validation of stability indicating RP-HPLC method for the determination of ezetimibe in pharmaceutical dosage forms

... The specifici- ty of the method was determined by assessing interference from the placebo and by stress testing of the drug (forced degradation).The developed method was validated in ter[r] ...

1

Development and validation of a genome scale metabolic model for the malolactic bacterium oenococcus oeni

Development and validation of a genome scale metabolic model for the malolactic bacterium oenococcus oeni

... a method associated to Pathway Tools, called “multiple gap filling”, which suggests corrections to different model components (reactions, metabolites, nutrients or secretions) to allow the model to ...this ...

158

Development and validation of the Statistical Anxiety Scale

Development and validation of the Statistical Anxiety Scale

... the method known as Minimum Rank Factor Analysis (ten Berge & Kiers, ...MRFA method has the advantage of distinguishing the common variance explained from the total common variance, hence making it ...

7

Development and validation of a method to determine amoxicillin in physiological fluids using micellar liquid chromatography

Development and validation of a method to determine amoxicillin in physiological fluids using micellar liquid chromatography

... selectivity and asymmetry in ...phase, and would also lead to the formation of an anionic hydrophilic layer, which would explain the high resolution achieved by SDS for hydrophilic ...

24

Evaluating Resilience: Development and validation of the Situated Subjective Resilience Questionnaire for Adults (SSRQA).

Evaluating Resilience: Development and validation of the Situated Subjective Resilience Questionnaire for Adults (SSRQA).

... positively and nega- tively worded items, thus these items often form two separate factors, even when their content is ...positively and negatively worded items because they are sensitive to the apparent ...

13

Development and validation of LC-ESI-MS method for the quantification of dapoxetine in rat plasma

Development and validation of LC-ESI-MS method for the quantification of dapoxetine in rat plasma

... A sensitive and simple liquid chromatography/electrospray mass spectrometry (LC-ESI-MS) method for determination of dapoxetine in rat plasma using one-step protein precipitation was deve[r] ...

1

Development and validation of a RP-HPLC method for determination of citicoline monosodium in human plasma

Development and validation of a RP-HPLC method for determination of citicoline monosodium in human plasma

... The active drug was isocratically eluted at a flow rate of 1 ml/min at ambient temperature in a nucleosil C18 analytical column with a mobile phase composed of tetrabutyl ammonium hydrog[r] ...

1

Development and validation of an UV-spectrophotometric method for the dissolution studies of sitagliptin tablets

Development and validation of an UV-spectrophotometric method for the dissolution studies of sitagliptin tablets

... The method was ap- plied for the determination of the drug in commercial tablet preparations and proved to be reliable for quantification It was also used for the comparison of dissoluti[r] ...

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