4.14 Requerimiento de instalaciones y equipos
4.14.1 Área y terreno
The re ults of Pt vapor deposition on the HOPG(0001) surface and subsequent O2, CO and H2 are summarized as follows:
2-D/3-D particles ith an average height of 0.2-0.3 nm. A small part of the particles decorates the
or 0.2 ML Pt increased to 0.5 nm and after additional anneal g for 3 h to 0.6 nm.
for 1 h, the apparent average particle height of 0.7- 0.9 nm was observed. After annealing for an additional 6 h under identical g
the apparent average particle height was centered at ca. 0.5 nm. Prolon ed annealing for 9 h (total) resulted in an increase of the average particle
y occur by coalescence.
s
annealing in UHV,
1. Platinum deposited on the HOPG(0001) surface in the coverage range of 0.2-0.4 ML initially forms randomly distributed and irregularly shaped
w
step edges of the substrate. Annealing the Pt (0.3 ML)/HOPG system in UHV (7 h total) results in the formation of a very narrow Pt particle size distribution centered at 0.5-0.6 nm.
2. After annealing in oxygen, p(O2)=2×10–5 mbar for 1 h at 500 °C, the average height of the particles f
in
3. After annealing the Pt(0.4 ML)/HOPG sample in the presence of CO, p(CO)=2×10–5 mbar at 500 °C
conditions, the average size of the particles increased to 1.3-1.5 nm. Particles of a lobular morphology were found to assemble into aggregates consisting of several separate particles. Very strong decoration of step edges with spherical particles was found.
4. After annealing the sample with 0.2 ML of Pt in H2, p(H2)= 2×10–5 mbar at 500 °C for 1 h
g
height to 0.8 nm. The histograms of particles height distributions exhibited two peaks in the range of ca. 0.5-1.0 nm. In addition to these particles, smaller particles with an apparent height of 0.2-0.3 nm have been registered.
5. The annealing experiments in UHV and gaseous environment (O2, CO and H2) indicate that in all the cases the growth of Pt nanoparticles ma
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