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The IS. coli export pathway has been analysed using a combination of

genetic, biochemical and physiological techniques. Table 1.1. lists the known

components of the j!. coll export apparatus and their putative modes of

action.

A genetic approach was used to isolate mutants defective in protein

export. The approaches taken have recently been reviewed (Bieker and

Silhavy, 1990) and are described below. Hybrid proteins were constructed

between the 3' region of the lacZ gene of E. coii and the 5' end (containing

the signal-sequence encoding DNA) of genes encoding for the normally

exported proteins maiE and lamB. The hybrid proteins (MalE-LacZ and

LamB-LacZ) were targeted to the IM of _E. coll and their production was

Induced by maltose. The fusion proteins were recognised by the export

apparatus but could not complete the process because the J3-galactosidase

molecule adopted a conformation that could not be exported. This led to an

Inactive p-galactosldase (because it was unable to form functional

tetramers) and also resulted in the jamming o f the export apparatus. High

levels of production o f either of these hybrid proteins (controlled by maltose

levels) were lethal as they completely jammed the export apparatus. When

these fusions were introduced into a lac

A

strain of E. coli, the resulting phenotype was Lac- and Mals. Maltose resistant (Malr) mutants were then

searched for In order to identify intragenic targeting signals for the fusion

proteins. Such mutants would not target the hybrid protein to the IM and

therefore would not jam the export machinery. Indeed, the vast majority of

the mutations (conferring Malr) were located in the signal-sequence of the hybrid proteins.

Three approaches were then taken -to identify components of the

export apparatus. The first approach was to identify extragenlc suppressors of

Table 1.1. Components of the ji. coli protein export apparatus

Protein Location Size

(kD)

Function

SecB Cytoplasm

12

Form complexes with pre-

Trigger factor 60 proteins to maintain

GroEL 910 translocation competence

[Chaperones]

SecA Membrane

(peripheral)

102

ATPase, directs [pre- protein/chaperone] complex to IM

SecY Membrane 49 Interact with SecA,

SecE (integral) 14 translocators?

Lep Membrane 36 Process pre-proteins

LspA (integral) 18 Process pre-lipoproteins

SecD Membrane 65 Unknown, late step in

SecF (integral) 35 translocation?

Legend

The information for this table was obtained from the following sources; Bieker and Silhavy, (1990); Bassford et al., (1991), Lecker et al., (1989) and Crooke et al., (1988).

signal-sequence mutations. Strains carrying mutations in the signal-sequences

of either MalE or LamB were used. Restoration of the Mal+ phenotype was

sometimes produced by mutations in export proteins which interacted with

the (mutated) signal-sequence of MalG or LamB. These genes were termed

prl as they were involved in protein localisation. Three genes were identified

which were called prlA, prlD and prlG. Surprisingly, the £rl mutations were

not lethal even though they were in essential genes.

The second approach taken led to the identification of the sec genes,

some of which were allelic with £rl genes. In this approach general export

defects were screened for in the fusion protein (MalE-LacZ) in a

lacA background (as described earlier). Secretion mutants of the above

strain were identified on the basis of increased ^-galactosidase activity at

30°C. The production of an active p-galactosidase was in some cases

expected to result from mutations in the export machinery. Such mutations

would cause an inability of the export apparatus to recognise the

signal-sequence of the MalE-LacZ protein which would then reside (and form

active molecules) within the cytoplasm. Such mutants were then re-screened

for a conditionally lethal phenotype. This approach was used to identify secA

and secB. A similar approach, using PhoA-LacZ and LamB-LacZ fusions, was

used to identify secD and secE.

The third approach came from findings that secA gene expression was

de-repressed under conditions that inhibited protein export. A SecA-LacZ

fusion was constructed (in a merodiplold containing secA-*-) and conditional

lethal mutants were Isolated with raised levels o f p-galactosidase activity.

This approach led to the discovery of secE. (cold-sensitive). Mutations were

mutations in secB were isolated because secB mutations do not cause over-

expression of secA.

Biochemical studies have focussed on isolating the components of the

export apparatus. The reconstitution of an hi vitro synthesis/transport system

then followed which enabled the study o f the individual components of the

export apparatus. The in vitro system has relied heavily on the use of

inverted plasma membrane vesicles. Under the correct conditions and with

the necessary components it is possible to direct various, normally exported,

proteins into such vesicles (Swidersky et al., 1990). Once proteins are

internalised into vesicles they are immune from proteinase attack. This

feature can serve as an assay to monitor the progress of protein

translocation. This type of experiment has been used to demonstrate the

necessity of SecA (Swidersky et al., 1990, Cunningham et al., 1989), SecB

(Watanabe and Blobel, 1989) and SecY/E (Brundage £t al., 1990) in protein

export. A summary of the components o f the jl. coli export machinery and

their proposed functions is shown in Table 1.1. and described below.

The translocation of proteins across the IM of IS. coll involves several

cytoplasmic and membrane protein factors (see above). These include six sec

gene products (SecA [PrlD], SecB, SecD, SecE [PrlG], SecF, SecY [PrlA ]) and

signal-peptidase(s). Other proteins, as well as the Sec proteins, have been

implicated in the export of some classes o f protein. Trigger factor has been

demonstrated to be needed for the in vitro 'export' o f pre-OmpA into

E. coli IM vesicles (Crooke and Wickner, 1987). The E. coll heat shock

proteins, GroEL and GroES, have also been implicated in protein export in

E. coli (Rusukawa et al., 1989).

Biochemical approaches have been used to analyse the functions of

SecA and SecB and have been reviewed (Bieker and Silhavy, 1990). An

elaborate genetic approach, termed suppressor-directed inactivation (SDI),

was used to investigate SecY and SecE. The LamB-LacZ hybrid protein with a

defective signal was used in a merodiploid £ . coli strain carrying a

suppressing SecE (recognising the mutated LamB-LacZ signal-sequence)

protein and SecE+. The cell functions normally because the SecE+ protein

does not recognise (and is not blocked by) the mutant hybrid protein. The

hybrid protein is, however, trapped by the mutated (suppressing) SecE. The

suppressor directed inactivation step can be studied to identify the stage of

the block. The signal-sequence of The LamB-LacZ protein was not processed

when blocked at the stage of action o f SecE. However, when blocked at

SecY, the protein had been processed. This indicated that SecY functioned at

a later stage in the export pathway than SecE. Recent work has suggested

that a truncated version of SecE is functional (Schatz et al., 1991). The

SecE truncate had only one of three membrane-spanning domains remaining

and this was sufficient for its function.

In addition to these proteinaceous factors, ATP (Lill et al., 1989) and

the proton motive force (Schiebel et al., 1991) are also required for protein

export across the _E. coll inner-membrane (IM ).